SCHEDULED MAINTENANCE
The reaction between solid (NMP)n{[BiBr4]}n (1) (NMP = N-methylpyridinium) and Br2, generated in situ in HBr solution, results in the formation of (NMP)3[Bi2Br9]·Br2 (2). In the structure of 2, dibromine molecules connect discrete binuclear [Bi2Br9]3− anions into an extended network. Complex 2 is thermally stable (up to 150 °C).
S. A. Adonin, I. D. Gorokh, P. A. Abramov, P. E. Plyusnin, M. N. Sokolov and V. P. Fedin, Dalton Trans., 2016, 45, 3691 DOI: 10.1039/C5DT04464B
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